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Document Details
Document Type
:
Article In Journal
Document Title
:
Synthesis and spectroscopic studies of complexes containing the Schiff base 1-acetylferrocene(thio)s
Synthesis and spectroscopic studies of complexes containing the Schiff base 1-acetylferrocene(thio)s
Document Language
:
Arabic
Abstract
:
[RuCl2(CO)(2)](n) reacts with the Schiff base 1-acetylferrocenethiosemicarbazone, [Fe(eta-Cp)(eta-C(5)H(4)MeC=NNHCSNH2)] to give [Fe(eta-Cp)(eta-C(5)H(4)MeC=NNHCSNH2)RuCl2(CO)(2)] and with 1-acetylferrocenesemicarbazone [Fe(eta-Cp)(eta-C(5)H(4)MeC=NNHCONH2)] to give [Fe(eta-Cp)(eta-C(5)H(4)MeC=NNHCONH2)RuCl2(CO)(2)]. Spectroscopic data indicate that the Schiff bases act as bidentate ligands and coordinate to ruthenium via the hydrazinic N and either the S or O atoms, respectively, giving stable heterobimetallic complexes, which have been characterized by i.r. and H-1-n.m.r. spectroscopies, and elemental analyses.
Journal Name
:
TRANSITION METAL CHEMISTRY
Volume
:
21
Issue Number
:
1
Publishing Year
:
1996 AH
Added Date
:
Saturday, June 14, 2008
Researchers
Researcher Name (Arabic)
Researcher Name (English)
Researcher Type
Dr Grade
Email
أحمد عمر بغلف
Researcher
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