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Document Details
Document Type
:
Article In Journal
Document Title
:
NEW COMPLEXES OF RUTHENIUM(II) WITH THIOSEMICARBAZIDE AND BETA-DIKETONE LIGANDS
NEW COMPLEXES OF RUTHENIUM(II) WITH THIOSEMICARBAZIDE AND BETA-DIKETONE LIGANDS
Document Language
:
Arabic
Abstract
:
The reaction of thiosemicarbazide (NH2.NH.CS.NH2) with [Rh(CO)2Cl2]n in THF gives an air stable, off white solid Ru(CO)2Cl2.NH2.NH.CS.NH2. The ligand acts as bidendate and its has been suggested that it coordinates to the metal through N(1) and S atom. Also the salt [Ru(CO)2Cl2]n reacts with an excess of sodium acetylacetonate in THF and gives very stable red solid Ru(CO)2(acac)2xH2O. Similar product is obtained when [Ru(CO)2Cl2]n is treated with acetylacetone in presence of a base such as triethylamine. The complexes were characterised by IR, NMR and elemental analyses.
Journal Name
:
JOURNAL OF THE CHEMICAL SOCIETY OF PAKISTAN
Volume
:
12
Issue Number
:
3
Publishing Year
:
1990 AH
Added Date
:
Saturday, June 14, 2008
Researchers
Researcher Name (Arabic)
Researcher Name (English)
Researcher Type
Dr Grade
Email
أحمد عمر بغلف
Researcher
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